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Journal article
The natural constituents of historical textile dyes
The sources and structures of dyes used to colour Western historical textiles are described in this tutorial review. Most blue and purple colours were derived from indigo—obtained either from woad or from the indigo plant—though some other sources (e.g. shellfish and lichens) were used. Reds were often anthraquinone derivatives obtained...Ferreira, Ester S B ; Hulme, Alison N ; McNab, Hamish ; Quye, Anita
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Journal article
Probing the factors which control degradation in museum collections of cellulose acetate artefacts
Cellulose acetate artefacts in museum collections cover a period from the early 1900's to the present day. Conservators have observed that certain of these objects are showing signs of warping, crazing, cracking, discolouration and shrinkage accompanied by a strong smell of acetic acid. Previous studies on cellulose nitrate artefacts show...Ballany, Jane M ; Littlejohn, D ; Pethrick, R P ; Quye, Anita
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Journal article
Analytical studies of the degradation of cellulose nitrate plastics in museums
This paper discusses a project which is examining the degradation of cellulose nitrate artefacts. Several analytical techniques including Fourier transform infrared (FTIR) spectroscopy and ion chromatography have been used to investigate the degradation processes occurring and the various factors influencing the rate of degradation. Accelerated ageing of cellulose nitrate has...Stewart, R ; Littlejohn, D ; Pethrick, R P ; Quye, Anita ; Tennent, N H
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Journal article
Saving our polyesterdays: historical plastics research
Preventing the degradation of materials in museums has always been a challenge. Now plastics in 20th century museum artefacts are presenting a new set of problems.Quye, Anita
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Journal article
Negative ion electrospray mass spectrometry of neoflavonoids
The electrospray ionisation mass spectra of the neoflavanoids brazilin and hematoxylin are reported in both their reduced (1 and 2, respectively) and their oxidised forms (3 and 4, respectively). In the reduced forms, breakdown pathways under collision induced decomposition (CID) conditions produce fragments characteristic of rings A and C; in...Hulme, Alison N ; McNab, Hamish ; Peggie, David A ; Quye, Anita
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Journal article
2',4',6'-Trihydroxy-1-methoxyacetophenone monohydrate at 150 K
The geometry of the title compound, 2-methoxy-1-(2,4,6-trihydroxyphenyl)ethanone, C9H10O5·H2O, is determined by the presence of an intramolecular hydrogen bond; the geometry of the benzene ring is distorted by a flanking carbonyl group.Ferreira, Ester S B ; Hulme, Alison N ; McNab, Hamish ; Quye, Anita ; Parsons, S
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Journal article
Liquid chromatography determination of natural dyes in extracts from historical Scottish textiles excavated from peat bogs
Textiles excavated from Scottish sites belonging now to the collections of the National Museums of Scotland, including seventeenth century textiles from peat bogs in the Scottish Highlands and Islands, were selected for analysis by high performance liquid chromatography with photodiode array detection (PDA HPLC) to detect whether any dyes remained...Surowiec, Izabella ; Trojanowicz, Marek ; Quye, Anita
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Journal article
Raman spectroscopy of coloured resins used in antiquity: dragon's blood and related substances
Dragon's blood is a deep red resin which has been used for centuries by many cultures and much prized for it's rarity, depth of colour and alchemical associations. The original source of dragon's blood resin is believed to be Dracaena cinnabari from Socotra in Africa, but since mediaeval times there...Edwards, Howell G M ; de Oliviera, Luiz Fernando C ; Quye, Anita
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Journal article
‘Dragon’s Blood’ I—characterization of an Ancient resin using Fourier transform Raman spectroscopy
Several resins generically known as ‘dragon’s blood’ from different botanical and geographical sources were characterised non‐destructively using Fourier transform Raman spectroscopy. Genuine ‘dragon’s blood’ resin (Dracaena spp.) as found on Socotra Island was the probable source in antiquity. The spectra of recently collected Socotran resins from different sites were compared...Quye, Anita ; Edwards, Howell G M ; Farwell, D W
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Quye, Anita
lac, analysis, liquid chromatography, dyes, madder, Cochineal, and kermes
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Book chapter
The analytical characterisation of flavonoid photodegradation products: a novel approach to identifying natural yellow dyes in ancient textiles
In a previous study new compounds were detected from light aged natural yellow (flavonoid) dyes on alum mordanted wool. We have now developed a novel technique - negative ion electrospray ionisation quadrupole ion trap tandem mass spectrometry (ESI QIT MS) - for futher study and identification of characteristic flavonoid photodegradation... -
Book chapter
A preliminary study of light-ageing effects on the analysis of natural flavonoid-dyed wools by PDA HPLC and by DTMS
Initial results from high performance liquid chromatographic (HPLC) analysis of accelerated fluorescent tube- and mercury-incandescent lamp-aged mordanted wools dyed with old fustic, weld, quercitron bark, quercetin, dyer's greenweed and onion skins indicate that additional chromophoric and non-chromophoric compounds are generated upon photodegredation. Greater amounts of these componenets were generated after...
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