Busca
Resultados da Busca
-
Quye, Anita
lac, analysis, liquid chromatography, dyes, madder, Cochineal, and kermes
-
Journal article
Raman spectroscopy of coloured resins used in antiquity: dragon's blood and related substances
Dragon's blood is a deep red resin which has been used for centuries by many cultures and much prized for it's rarity, depth of colour and alchemical associations. The original source of dragon's blood resin is believed to be Dracaena cinnabari from Socotra in Africa, but since mediaeval times there...Edwards, Howell G M ; de Oliviera, Luiz Fernando C ; Quye, Anita
-
Journal article
Simulation experiments for determining the use of ancient pottery vessels: the behaviour of epicuticular leaf wax during boiling of a leafy vegetable
Laboratory experiments were performed using replica ceramic jars to simulate ancient pottery vessel use. The aim of the study was to investigate the behaviour of lipids, specifically, epicuticular leaf wax components during the processing of foodstuffs in unglazed ceramic vessels to determine if the pattern of lipid accumulation in a... -
Journal article
‘Dragon’s Blood’ I—characterization of an Ancient resin using Fourier transform Raman spectroscopy
Several resins generically known as ‘dragon’s blood’ from different botanical and geographical sources were characterised non‐destructively using Fourier transform Raman spectroscopy. Genuine ‘dragon’s blood’ resin (Dracaena spp.) as found on Socotra Island was the probable source in antiquity. The spectra of recently collected Socotran resins from different sites were compared...Quye, Anita ; Edwards, Howell G M ; Farwell, D W
-
Journal article
Liquid chromatography determination of natural dyes in extracts from historical Scottish textiles excavated from peat bogs
Textiles excavated from Scottish sites belonging now to the collections of the National Museums of Scotland, including seventeenth century textiles from peat bogs in the Scottish Highlands and Islands, were selected for analysis by high performance liquid chromatography with photodiode array detection (PDA HPLC) to detect whether any dyes remained...Surowiec, Izabella ; Trojanowicz, Marek ; Quye, Anita
-
Journal article
Negative ion electrospray mass spectrometry of neoflavonoids
The electrospray ionisation mass spectra of the neoflavanoids brazilin and hematoxylin are reported in both their reduced (1 and 2, respectively) and their oxidised forms (3 and 4, respectively). In the reduced forms, breakdown pathways under collision induced decomposition (CID) conditions produce fragments characteristic of rings A and C; in...Hulme, Alison N ; McNab, Hamish ; Peggie, David A ; Quye, Anita
-
Journal article
2',4',6'-Trihydroxy-1-methoxyacetophenone monohydrate at 150 K
The geometry of the title compound, 2-methoxy-1-(2,4,6-trihydroxyphenyl)ethanone, C9H10O5·H2O, is determined by the presence of an intramolecular hydrogen bond; the geometry of the benzene ring is distorted by a flanking carbonyl group.Ferreira, Ester S B ; Hulme, Alison N ; McNab, Hamish ; Quye, Anita ; Parsons, S
-
1992
-
1991
-
Journal article
Saving our polyesterdays: historical plastics research
Preventing the degradation of materials in museums has always been a challenge. Now plastics in 20th century museum artefacts are presenting a new set of problems.Quye, Anita
-
Journal article
Probing the factors which control degradation in museum collections of cellulose acetate artefacts
Cellulose acetate artefacts in museum collections cover a period from the early 1900's to the present day. Conservators have observed that certain of these objects are showing signs of warping, crazing, cracking, discolouration and shrinkage accompanied by a strong smell of acetic acid. Previous studies on cellulose nitrate artefacts show...Ballany, Jane M ; Littlejohn, D ; Pethrick, R P ; Quye, Anita
-
Journal article
Analytical studies of the degradation of cellulose nitrate plastics in museums
This paper discusses a project which is examining the degradation of cellulose nitrate artefacts. Several analytical techniques including Fourier transform infrared (FTIR) spectroscopy and ion chromatography have been used to investigate the degradation processes occurring and the various factors influencing the rate of degradation. Accelerated ageing of cellulose nitrate has...Stewart, R ; Littlejohn, D ; Pethrick, R P ; Quye, Anita ; Tennent, N H
-
Journal article
The natural constituents of historical textile dyes
The sources and structures of dyes used to colour Western historical textiles are described in this tutorial review. Most blue and purple colours were derived from indigo—obtained either from woad or from the indigo plant—though some other sources (e.g. shellfish and lichens) were used. Reds were often anthraquinone derivatives obtained...Ferreira, Ester S B ; Hulme, Alison N ; McNab, Hamish ; Quye, Anita
-
Journal article
Characterisation of ‘bog butter’ using a combination of molecular and isotopic techniques
The chemical analyses of ‘bog butters’ recovered from peat bogs of Scotland were performed with the aim of determining their origins. Detailed compositional information was obtained from ‘bog butter’ lipids using high temperature gas chromatography (HTGC) and GC-mass spectrometry (GC-MS). The results indicate the degree to which ‘bog butters’ have...Berstan, Robert ; Dudd, Stephanie N ; Copley, Mark S ; Morgan, E David ; Quye, Anita …
-
Journal article
The practice of dyeing wool in Scotland c.1790-c.1840
The history of dyeing is complex, even when analysed over a short period of time and in a comparatively small country such as Scotland. There are hundreds of dyes, natural and manufactured; most require the use of further chemicals as mordants to fix the colour; dyes interact with different vegetable...Burnett, John ; Mercer, Katherine ; Quye, Anita
-
2008
Journal article
Rediscovering the Arisaid
The stereotype of 'traditional' Highland dress is the kilted male figure. The National Museums Scotland (NMS) and other museums have long included a category 'Arisaids' in their collections; research reveals that this was a female version of 'traditional' Highland dress, a finely-made and high status garment which was going out...Quye, Anita ; Cheape, Hugh
-
2009
Journal article
Negative ion ESI–MS analysis of natural yellow dye flavonoids : an isotopic labelling study
Flavonoids are amongst the most commonly used natural yellow colourants in paintings, as lakes, and in historical textiles as mordant dyes. In this paper, evidence from isotopically labelled substrates is used to propose negative ion electrospray collision induced decomposition mechanisms of flavones, flavonols and an isoflavone. These mechanisms include a...McNab, Hamish ; Ferreira, Ester S B ; Hulme, Alison N ; Quye, Anita
Flavonoids , Historical textiles, Lake pigments, and Electrospray
-
2011
Journal article
Investigation of inherent degradation in cellulose nitrate museum artefacts
Cellulose nitrate was one of the first semi-synthetic plastics to be commercially exploited and as such many museums contain a large number of artefacts illustrating the versatility of this plastic for the creation of a wide variety of functional and aesthetic artefacts. Conservators find themselves faced with the challenge of...Quye, Anita ; Littlejohn, D ; Petherick, R ; Stewart, R
-
2013
Journal article
Investigation of the degradation of cellulose acetate museum artefacts
Cellulose acetate artefacts from various museums have been analysed by micro-FTIR spectrometry and ion chromatography in an attempt to identify whether there are any common factors associated with their degradation. There was good correlation between the IR spectra, the concentration of ions extracted from an artefact and the visual degree...Littlejohn, D ; Petherick, R ; Quye, Anita ; Ballany, Jane M