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2023
Journal article
Historical Textile Dye Analysis Using DESI-MS
Desorption electrospray ionization mass spectrometry (DESI-MS) is an ambient mass spectrometry technique that shows great potential for the analysis of fragile heritage objects in situ. This article focuses on the application of a recently built DESI source to characterize natural dyestuffs in historical textiles and a presentation of initial imaging...Sandström, Edith ; Vettorazzo, Chiara ; Mackay, C Logan ; Troalen, Lore G ; Hulme, Alison N
mass spectrometry, mass spectrometry imaging, natural dyes, non-invasive analysis, and textile
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2023
Journal article
Pests or prey? Micromammal species within an ancient anthropic environment at the Norse settlement site of Tuquoy (Westray, Orkney)
Micromammals, like rodents and shrews, adapt rapidly to take advantage of new food sources, habitats and ecological niches, frequently thriving in anthropogenic environments. Their remains, often retrieved during archaeological investigations, can be a valuable source of information about the past environmental conditions as well as interspecies interactions and human activity....Romaniuk, Andrzej A ; Troalen, Lore G ; Bendrey, Robin ; Herman, Jeremy S ; Owen, Olwyn …
commensalism, introductions, Orkney, micromammal, archaeology, and predation
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2023
Journal article
Development and Application of Desorption Electrospray Ionization Mass Spectrometry for Historical Dye Analysis
A desorption electrospray ionization (DESI) source was built and attached to a Bruker 7T SolariX FT-ICR-MS for the in situ analysis of 14 early synthetic dyestuffs. Optimization using silk and wool cloths dyed with rhodamine B concluded that when using a commercial electrospray emitter (part number: 0601815, Bruker Daltonik), a...Sandström, Edith ; Vettorazzo, Chiara ; Mackay, C Logan ; Troalen, Lore G ; Hulme, Alison N
Solvents, Dyes and pigments, Biomimetic materials, Ions, and Fibers
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2021
Journal article
An optimised small-scale sample preparation workflow for historical dye analysis using UHPLC-PDA applied to Scottish and English Renaissance embroidery
A sample preparation workflow for historical dye analysis based on 96 well plates and filtration by centrifugation was developed. It requires less sample and the introduced error is decreased, making it useful for culturally important objects. A sample preparation workflow for historical dye analysis requiring less sample has been developed....Sandström, Edith ; Wyld, Helen ; Mackay, C Logan ; Troalen, Lore G ; Hulme, Alison N